栀子黄制备工艺及鹅绒藤化学成分分析-preparation technology of gardenia yellow and analysis of chemical composition of goose down vine.docx

栀子黄制备工艺及鹅绒藤化学成分研究 英文摘要chinense and elucidated as n-hexadecanioc acid (1), salicylic acid (2), β-sitosterol (3),β-sitosterolglucoside (4), apigenin (5), kaemperol (6), kaemperol-3-O-β-D-glunoside (7),tricin (8), and tricin-7-O-β-D-glucuronide (9). Compounds 5, 8 and 9 were obtained from this genus for the first time. A method was developed to quantitative analysis of tricin-7-O-β-D-glucuronide and astragalin in this herbal material, which was determined to be 2733 and 69.67 μg/g for tricin-7-O-β-D-glucuronide and astragalin, respectively. These results have laid the foundation for further exploring the active ingredients and quality control of Cynanchum chinense R. Br.Keywords: gardenia jasminoides; gardenia yellow; crocin; geniposide; macroporous resin; reversed-phase medium pressure liquid chromatography; cynanchum chinense; tricin-7-O-β-D-glucuronideWrittenby Jiang-Yong FengSupervised by Gui-Zhen Ao (Associate Professor)Jiang-Yun Liu (Associate Professor)III目录引言 ............................................................................................................................ 1第一章栀子研究进展 ................................................................................................... 21.1栀子研究与开发概况........................................................................................ 21.1.1栀子化学成分及药理活性研究概况....................................................... 21.1.2栀子黄及栀子苷在天然色素中的应用 ................................................... 61.2栀子提取分离工艺研究进展 ............................................................................ 81.2.1栀子黄的提取 ......................................................................................... 81.2.2栀子黄及栀子苷的分离 .......................................................................... 91.3立题背景和意义 ..............................................................................................111.4本论文主要研究内容.......................................................................................11第二章栀子黄制备工艺研究....................