Tool bar and button bar (Many SEM functions are mouse 工具条和按钮栏（许扫描功能的鼠标.pptVIP

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2018-06-19 发布于福建
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Tool bar and button bar (Many SEM functions are mouse 工具条和按钮栏（许扫描功能的鼠标.ppt

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Tool bar and button bar (Many SEM functions are mouse 工具条和按钮栏（许扫描功能的鼠标

Tool bar and button bar(Many SEM functions are mouse-controlled) To insert your sample Check that high voltage (HV) is off (no yellow background) Click on Vent Insert sample. Wear gloves or use tools. Check sample height with “elephant nose”. Bottom of nose is where highest point on sample should be. Click on quadrant showing CCD image (typically lower right) Make sure image is live, not paused! (No double green bars in upper right corner.) Slowly close door while watching monitor to assure that sample/holder is clear of pole piece and detector Click on “Pump” with left hand while holding door shut with right hand. Check that door is shut! Push top of door against chamber. Before pumpdown: get oriented With the door open Move the stage to be under the beam: X=0, y=0 “Control zero” is also supposed to work Enter positive and negative values for x and y Observe and record the direction the stage moves Perform a similar operation after you get an image to correlate directions on screen to directions on the sample Magnetic hazards Ferromagnetic particles are potentially the most dangerous thing you can image If they get sucked into the column, the rebuild will cost $60-100k! Trying to image loose ferromagnetic particles in immersion mode will be fatal!!! They can be imaged in EDX mode They can be imaged in immersion mode if firmly embedded in plastic. Do not use tape!! Getting started toward an image When adequate vacuum has been reached, chamber icon becomes green and HV button changes from grey to black. Click on HV! Get an image! Black screen: Check that H(igh) V(oltage) is on: yellow background? HV automatically shuts off when switching between High Vac and Low Vac! Turn on waveform feature Increase contrast and brightness so waveform fills region between lines Go to minimum magnification Can you see the aperture? If not, you are in big trouble. Check HV! Try spot size = 4, 15 kV Link Initially your stage should be about 13 mm down if you have not rais