石墨炉原子吸收培训课程之五.pptVIP

下载本文档

16
0
约5.39千字
约 29页
2018-06-21 发布于河南
举报
版权申诉

石墨炉原子吸收培训课程之五.ppt

1、本文档共29页，可阅读全部内容。
2、原创力文档（book118）网站文档一经付费（服务费），不意味着购买了该文档的版权，仅供个人/单位学习、研究之用，不得用于商业用途，未经授权，严禁复制、发行、汇编、翻译或者网络传播等，侵权必究。
3、本站所有内容均由合作方或网友上传，本站不对文档的完整性、权威性及其观点立场正确性做任何保证或承诺！文档内容仅供研究参考，付费前请自行鉴别。如您付费，意味着您自己接受本站规则且自行承担风险，本站不退款、不进行额外附加服务；查看《如何避免下载的几个坑》。如果您已付费下载过本站文档，您可以点击这里二次下载。
4、如文档侵犯商业秘密、侵犯著作权、侵犯人身权等，请点击“版权申诉”（推荐），也可以打举报电话：400-050-0827(电话支持时间：9:00-18:30)。
5、该文档为VIP文档，如果想要下载，成为VIP会员后，下载免费。
6、成为VIP后，下载本文档将扣除1次下载权益。下载后，不支持退款、换文档。如有疑问请联系我们。
7、成为VIP后，您将拥有八大权益，权益包括：VIP文档下载权益、阅读免打扰、文档格式转换、高级专利检索、专属身份标志、高级客服、多端互通、版权登记。
8、VIP文档为合作方或网友上传，每下载1次，网站将根据用户上传文档的质量评分、类型等，对文档贡献者给予高额补贴、流量扶持。如果你也想贡献VIP文档。上传文档

石墨炉原子吸收培训课程之五

Improving Productivity in GFAA Fast Furnace Slurry Sampling EPA Method 200.9 Graphite Furnace AA Analysis 客戶需求 Maximum sample throughout Low cost per analysis Exceptional analytical performance Accurate and reliable result Easy to use instrument system Simplified compliance with quality control protocols Quality, reliability and support The Answer : SIMAA 6100 多可同時最多分析 6種元素加熱系統 Transversely Heated Graphite Atomizer (THGA) 穩定溫度平台 Stabilized Temperature Platform Furnace (STPF) 光學系統 Tetrahedral Echelle Polychromator (TEP) 背景較正系統 Longitudinal Zeeman Background Corrector 偵測器 Solid State Detector SIMAA 6100Simultaneous Multielement Graphite Furnace AAS One Dimensional Dispersion Two Dimensional Dispersion Solid State Detector Simultaneous Analysis Fast Furnace Zeeman background correction accommodates relatively high background levels during atomization Using a Lvov platform eliminates many matrix interferences High light throughput spectrometers often have DLs that exceed many environmental lab requirements Fast Furnace Autosamplers can pipet accurately and with high precision at small volumes (5 ?L or less) Reduce background levels; decrease dry time Matrix modifiers can contribute background and contamination to an analysis Reduce background levels; decrease dry time Fast Furnace: Pb HGA Program Fast Furnace: Pb THGA Program Fast FurnacePb Using Continuum Background Correction Fast Furnace: Conclusions Fast furnace is one approach to improve throughput in a production lab environment If samples contain high concentrations of acids, dry time and temperature should be modified so that tube lifetime is not diminished Automated Solid Sampling in GFAA Slurry Sampling Slurry Sampling - General Procedure 1. Calibrate instrument using aqueous standards. 2. Weigh a homogeneous sample directly in the autosampler cup (usually 1-20 mg). 3. Add 1-1.5 mL suspending fluid (e.g., 5% HNO3 + 0.01% Triton-X) . 4. Adjust sonicating power and time such that the sample