DO-Measurement-溶解氧测量.pptVIP

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DO-Measurement-溶解氧测量.ppt

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The Measurement of Dissolved Oxygen YSI (Hong Kong) Ltd. Release 1.1 / 2000.01 YSI INCORPORATED Employee-Owned ISO-9001 Certified ISO-14001 Certified Innovation (selected) 1952 First quartz crystal electronic stopwatch 1952 First medical electronic thermometer 1955 First interchang. thermistor temp. probe 1957 First commercial heart-lung machine 1957 First instantaneous blood-gas analyzer 1963 First practical dissolved oxygen meter 1965 First linear thermistor temperature sensor 1965 First polarographic biological oxygen monitor 1972 First immobilized-enzyme-activated polarographic sensor 1977 First gallium melting point temperature standard (29.7715oC) 1981 First superior-stable precision inter-changeable thermistor 1992 First long-term in-situ stirring-independent oxygen sensor 1993 First stirring-independent micro-electrode oxygen sensor 1996 First conductivity instrument using Resistance Ratio Tech- nology? for high accuracy measurement of ultrapure water Seminar Topics Where DO is Measured How DO is Measured Calibration New DO Applications Interferences and Precautions Care Maintenance WhereDissolved Oxygenis Measured Percentage of Elements(in Dry Air, by Volume) Nitrogen 78.06% Argon 0.93% Hydrogen 0.01% Helium 0.0005% Ozone 0.00006% Oxygen 20.99% Carbon dioxide 0.03% Neon 0.002% Krypton 0.0001% Xenon 0.000009% Oxygen Uptake Rate HowDissolved Oxygenis Measured Probe Reaction Cathode O2 + 2 H2O + 4 e– ?? 4 OH– Anode 4 Ag + 4 Cl– ?? 4 AgCl + 4e– Total O2 + 2 H2O + 4 Ag + 4 KCl ?? 4 KOH + 4 AgCl Factors AffectingDO Measurement Temperature Salinity Barometric Pressure Sample Flow Temperature ~3% per °C 160 mm Hg at 20°C = 20 μA 160 mm Hg at 15°C ? 17 μA Temperature Corrected 160 mm Hg at 20°C = 20 μA 160 mm Hg at 15°C ? 17 μA 160 mm Hg at 15°C = 20 μA T = 20°C Fresh Water 160 mm Hg at 20°C = 20 μA = 9.09 mg/L 160 mm Hg at 15°C = 20 μA ? 9.09 mg/L Needs solubility compensation Fresh Wate