kta醋酸甲酯羰基化合成醋酐工艺设计.docVIP

安徽建筑工业学院本科生毕业设计 PAGE \* MERGEFORMAT 2安徽建筑工业学院毕 业 设 计 (论 文)专 业 化学工程与工艺 班 级 07化工①班 学生姓名 @@@ 学 号 @@ 课 题 50kt/a醋酸甲酯羰基化合成醋酐工艺设计 指导教师 葛业君 2011年 6 月50kt/a醋酸甲酯羰基化合成醋酐工艺设计 PAGE \* MERGEFORMAT 1摘 要醋酐是一种重要的有机化工原料，主要作为乙酰化剂，也能用作脱水剂和溶剂等。本设计通过比较现有醋酐生产乙醛氧化联产法、醋酸裂解法和醋酸甲酯羟基合成法，醋酸甲酯羟基化法较其他两种方法具有流程短，产品质量好，消耗指标低，三废排放少等优点，代表了当前醋酐生产的先进技术潮流，国外发达国家普遍采用此技术生产醋酐。此工艺需要解决主要问题是实现CH3COOCH3和CO的高效合成。设计了醋酸甲酯羰基化合成醋酐的工艺流程进并对主要设备闪蒸器进行设计。关键词： 醋酐 化工原料 羰基化 闪蒸器 醋酸甲酯ABSTRACTVinegar anhydride is an important organic chemical raw materials, mainly as a acylation agent, and can be used as dehydrant and solvent, etc. This design by comparing existing vinegar anhydride acetaldehyde oxidation method, the joint production of acetic acid methyl acetate cracking method and hydroxyl synthesis, methyl acetate hydroxyl method is better than the other two methods have good quality of product, process short, low consumption, waste discharge index wait for few advantages, represents the current acetic anhydride was the advanced technology of production trend, widely used in developed countries as the technology production vinegar anhydride. This process needs to solve the main problem is to realize efficient synthesis CH3COOCH3 and CO. Design the methyl acetate carbonyl compounds into the process flow into the repayment period of the main equipment braising apparatus to carry on the design.Keywords: vinegar anhydride chemical raw materials hydroformylation braising apparatus methyl acetate目录 TOC \o 1-3 \h \z \u HYPERLINK \l _Toc295570861 摘 要 PAGEREF _Toc295570861 \h 1 HYPERLINK \l _Toc295570862 前言 PAGEREF _Toc295570862 \h 5 HYPERLINK \l _Toc295570863 第一章 文献综述 PAGEREF _Toc295570863 \h 7 HYPERLINK \l _Toc295570864 1.1 课题的工艺背景 PAGEREF _Toc295570864 \h 7 HYPERLINK \l _Toc295570865 1.1.1 课题的提出 PAGEREF _Toc295570865 \h 7 HYPERLINK \l _Toc295570866 1.1.2 研究目标 PAGEREF