纳米tio2中空纤维光催化材料模板法制备与改性-preparation and modification of nano tio _ 2 hollow fiber photocatalytic material template method.docxVIP

第二章TiO2中空纤维材料的模板法制备及其光催化性能研究262.1引言........................................................................................................262.2实验部分.................................................................................................272.2.1主要仪器与试剂.............................................................................272.2.2TiO2中空纤维结构光催化材料的制备282.2.3光催化性能的测试.........................................................................292.3结果与讨论.............................................................................................30TG分析30XRD分析31SEM分析33BET测试34XPS分析35UV-Vis分析362.3.7样品的光催化性能.........................................................................3模拟太阳光下样品S-1~7的光催化性能3煅烧温度对样品光催化活性的影响...................................3煅烧时间对样品光催化活性的影响...................................3暗态和紫外光下最佳样品S-t的光催化性能以及紫外光下MB的光解40最佳样品S-t的重复使用性能422.4本章小结.................................................................................................43参考文献........................................................................................................44第三章pH值和CTAB对TiO2中空纤维材料相结构、形貌及其光催化性能的影响483.1引言.........................................................................................................483.2实验部分...............................................................................................483.2.1主要仪器与试剂.............................................................................483.2.2样品的制备....................................................................................493.2.3光催化性能的测试.........................................................................503.3结果与讨论.............................................................................................50XRD分析504.1引言.........................................................................................................644.2实验部分.................................................................................................654.2.1主要仪器与试剂.........................................................