山核桃蒲鞣质提取纯化工艺及对羊毛染色性能分析-extraction and purification of tannins from carya cathayensis and analysis of dyeing properties of wool.docx

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2018-08-07 发布于上海
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山核桃蒲鞣质提取纯化工艺及对羊毛染色性能分析-extraction and purification of tannins from carya cathayensis and analysis of dyeing properties of wool.docx

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山核桃蒲鞣质提取纯化工艺及对羊毛染色性能分析-extraction and purification of tannins from carya cathayensis and analysis of dyeing properties of wool

AbstractInordertomakefulluseofcaryacathayensissarg,tanninswasextractedfromcaryacathayensissargpeelsandtheoptimumextractingmethodandconditionswerecomfirmedthroughsinglefactorandresponsesurfacemethods.Onthebasisofthis,integratedtechnologyofmembranetopurifyleachliquorofcaryacathayensissargpeelswereemployedwiththemethodsofmicrofiltration,ultrafiltrationandreverseosmosis,andthenspraydrying.Inthelast,theproductoftanninwasusedtodyethewoolfiber.ThecortexcharacteristicsandcuticularlayercharacteristicsofwoolfiberwereanalizedbySanningElectronMicroscope（SEM）beforeandafterdyedbytannin.Themainresultswereshownasfollows:Responsesurfacemethodologywasemployedtooptimizetheextractionconditionoftanninsfromcargacathayensissargpeelstreatedwithwater.Onthebasisofone-factor-at-a-timeexperiments,afour-factor,three-levelquadraticgeneralrotaryunitizationdesignwasemployedtoestablishaquadraticpolynomialmathematicalmodelthatdescribesextractingrateasafunctionoffourprocessconditions,andtheestablishedmodelwasanalyzedbydrawingresponsesurfaceandcontourplots.Theoptimalextractionconditionswere:extractiontime95min,temperature65℃,liquidratio1:16andmeshsize50.Undertheseconditions,thetanninyieldratiowas23.49mg/gandthepuritywas80.3%.Leachliquorofcargacathayensissargpeelswerefiltratedbyinorganicceramicmembraneandpolysulfonehollowfiberultrafiltrationmembranes,theeffectivecomponentwasenrichedandtheun-wantedlargmoleculeswereremovedinthismethod.Theoptimumoperationwerealsodeterminedintheseexperiments,suchastheinorganicceramicmembraneporediameter,theaverageinterceptmolecularweightofpolysulfonehollowfiberultrafiltrationmembranes.Theresultshowedthatthepurityoftanninsfromcargacathayensissargpeelscanreach80.3%ComparedwithHPLCchromatogramoftheproductoftanninofcargacathayensissargpeelsandHPLCchromatogramofleachliquorofcargacathayensissargpeels,analysetheeffectofspraydryingmethod.Theresultshowedthatspraydryingisaneffectivemethodfortanninsfromcargacathayensissargpeels.AHPLCdeterminationoftanninwasestablished.Tanninsweresepa