电感耦合等离子体原子发射光谱法测定食品-食品安全质量检测学报.PDFVIP

7 1 Vol. 7 No. 1 2016 1 Journal of Food Safety and Quality Jan. , 2016 * 吕小园 , 陈 练, 贺 鹏, 颜鸿飞, 张志荣 ( , , , 410004) 摘 要: 目的 (ICP-OES) 方法 , , 结果 0.5 mg/kg0.1 mg/kg0.1 mg/kg0.1 mg/kg , RSD5%, 90%~120%, 结论 , 关键词: ; ; ; ; ; ; Determination of Fe, Mn, Pb and Cd in food additive zinc sulphate by inductively coupled plasma optical emission spectrometry * LV Xiao-Yuan , CHEN Lian, HE Peng, YAN Hong-Fei, ZHANG Zhi-Rong (Hunan Entry-Exit Inspection and Quarantine Bureau, State Key Laboratory of Food Safety Testing, Hunan Key Laboratory of Food Safety Science Technology, Changsha 410004, China) ABSTRACT: Objective To establish a method for the determination of Fe, Mn, Pb and Cd in food additive zinc sulphate by inductively coupled plasma optical emission spectrometry (ICP-OES). Methods Samples were dissolved by water, and then the content of Fe, Mn, Pb and Cd was determined by ICP-OES using standard curve method. Results The detection limit of Fe, Mn, Pb and Cd in the sample was 0.5 mg/kg, 0.1 mg/kg, 0.1 mg/kg and 0.1 mg/kg, respectively. The results showed that this method had good precision (RSD5%, recovery rate 90%~120%) in line with the national standard. The results