基于动态微波辅助萃取法快速检测西红柿中六种三嗪类除草剂.PDF

5 5 Vol. 5 No. 5 2014 5 Journal of Food Safety and Quality May. , 2014 1 2 1* 1 张轶群 , 孙顺日 , 金海燕 , 丁 兰 (1. , 130012; 2. , 999093) 摘 要: 目的 方法 , , ; , , 0.5 mL; , -结果 , : 70%-, 350 W, 7 min, 1.0 mL/min, pH 8, , 2.0 g 1~1000 ng/mL , 0.995~0.998; 0.08~0.33 ng/g; 68%~104%, 5.0%~7.3%结论 , 关键词: ; -; ; Rapid detection of six triazine herbicides from tomatoes by dynamic microwave-assisted extraction method 1 2 1* 1 ZHANG Yi-Qun , SON Sunil , JIN Hai-Yan , DING Lan (1. College of Chemistry, Jilin University, Changchun 130012, China; 2. Kimchaek University of Technology, Pyongyang 999093, Korea) ABSTRACT: Objective A simple and fast sample pretreatment method was proposed for determination of triazine herbicides in tomatoes. Methods The triazine herbicides in tomato samples were extracted by dy- namic microwave-assisted extraction and puritied by salting liquid-liquid extraction method.