（毕业学术论文设计）-微波消解—原子吸收火焰法测定水菠菜中微量元素的研究.docVIP

PAGE PAGE 26 JIUJIANG UNIVERSITY 毕 业 论 文 题 目 微波消解—原子吸收火焰法测定水菠菜中微量元素的研究 英文题目 Microwave digestion - flame atomic absorption method for the determination of trace elements in water spinach 院 系 基础医学院药管系 班 级 姓 名 学 号 指导教师 二零一三年五月微波消解—原子吸收火焰法测定水菠菜中微量元素的研究 摘 要 目的: 探究水菠菜中微量元素Cu、Zn、Fe、Mn的含量。方法: 称取水菠菜样品三份。采用微波消解水菠菜，采用火焰原子吸收光谱法测定了水菠菜中的Cu、Zn、Fe、Mn的含量。结果: 水菠菜中铜的含量分别为2365 mg/kg、3272 mg/kg、3987 mg/kg, RSD为25.3%; 水菠菜中锌的含量分别为799.1 mg/kg、1030 mg/kg、1198 mg/kg, RSD分别为19.8%; 水菠菜中铁的含量分别为4806 mg/kg、6570 mg/kg、7874 mg/kg，RSD分别为24.0%; 水菠菜中锰的含量分别1607 mg/kg、2048 mg/kg、3197 mg/kg，RSD分别为35.6%。结论：微波消解法消化速度快，消化较彻底，元素损失很低，酸度易控制；原子吸收火焰光谱法测定水菠菜微量元素方法简便，本实验只是初步探索水菠菜中的微量元素。 【关键字】水菠菜; 微波消解;原子吸收火焰光谱法; 微量元素 Microwave digestion - flame atomic absorption method for the determination of trace elements in water spinach Abstract Objective: To explore the water spinach trace elements Cu, Zn, Fe, Mn content. Methods: Three samples of known water spinach were used. Water spinach using microwave digestion by flame atomic absorption spectrometric determination of water spinach Cu, Zn, Fe, Mn content. Results: The copper content in water spinach were 2365, 3272, 3987 mg/kg, respectively, and RSD was 25.3%. Water spinach zinc contents were 799.1, 1030, 1198 mg/kg, respectively. And RSD was 19.8%. Iron content of water spinach were 4806, 6570, 7874 mg/kg, respectively. RSD was 24.0%. Manganese contents in water spinach were 1607, 2048, 3197 mg/kg, respectively. RSD was 35.6%. Conclusion: Microwave digestion speed, more thorough digestion, elemental damage is very low, acidity easy to control; atomic absorption spectrometry water spinach trace method is simple, the present study is only a preliminary exploration of water spinach trace elements. 【Keywords】water spinach; microwave digestion; flame atomic absorption spectrometry; trace elements 目 录 TO