高效液相色谱法测定食品接触材料中丙烯酸酯类单体的迁移量.PDF

7 1 Vol. 7 No. 1 2016 1 Journal of Food Safety and Quality Jan. , 2016 * 李成发 , 李 英, 廖文忠, 陈旭辉, 孙小颖, 李泳涛, 白 爽 ( , 518067) 摘 要: 目的 12 方法 (EU)No. 10/2011, 3%10%20%50% , C18 (150 mm×4.6 mm, 5 µm), , 结果 12 0.3~60.0 mg/L()0.6~120.0 mg/L(), r2 0.999388.2%~109.3%, 1.19%~7.48%, 0.01~0.12 mg/L 0.03~0.24 mg/L 结论 , , , 12 , 6 , 关键词: ; ; ; Determination of migration amounts of acrylate monomers by high performance liquid chromatography in food contact materials * LI Cheng-Fa , LI Ying, LIAO Wen-Zhong, CHEN Xu-Hui, SUN Xiao-Ying, LI Yong-Tao, BAI Shuang (Shenzhen Entry-Exit Inspection and Quarantine Bureau, Shenzhen 518067, China) ABSTRACT: Objective To develop an effective analytical method for the simultaneous determination of migration amount of 12 kinds of acrylate monomers in food contact materials by high performance liquid chromatography (HPLC). Methods Aqueous food simulants (3% acetic acid, 10% ethanol, 20% ethanol, 50% ethanol) and fatty food simulant (isooctane) were used to soak food contact materials. The obtained simulants were separated on a C18 column(150 mm×4.6 mm, 5 µm). The results were qualitatively analyzed by retention time and quantit