《年产5万吨甲苯精制工段工艺设计》-毕业论文.docVIP

ANYANG INSTITUTE OF TECHNOLOGY 本 科 毕 业 设 计 年产5万吨甲苯精制工段工艺设计 Design of 50,000 t/a Toluene Refining Section 系（院）名称： 化学与环境工程学院 专业班级： 化学工程与工艺07级2班 学生姓名： 学 号： 200705020035 指导教师姓名： 指导教师职称： 讲师 2011年 5 月 年产5万吨甲苯精制工段工艺设计 摘要：苯和甲苯都是重要的有机化工原料，需要用精制来达到更高的纯度，以用来做为某些精细化学品的合成原料，苯与甲苯的分离一般采用精馏的方法进行。本文对50000t/a的甲苯精制工段进行设计，其主要工作为精馏塔的设计，包括物料衡算，热量衡算，工艺尺寸的设计，同时对具体操作参数及结构参数进行计算，获得泡点温度、理论塔板数、实际塔板数以及最小回流比等信息。该设计最后得到精馏塔塔径2.2m，塔高为19.2m，共29块塔板，塔板板间距为0.4m。其次文章对附属设备进行了计算与选型，确定了合适的塔顶冷凝器和塔底再沸器；最后综合生产质量及安全要求确定了工艺的控制体系。 关键字：精馏；甲苯；工艺流程设计；控制设置 Design of 50,000 t/a Toluene Refining Section Abstract: Benzene and toluene are important organic chemical raw materials. They need to achieve higher purity by refining so that they can be used as synthetic materials of some chemicals. Separation of benzene and toluene commonly used distillation methods. In this paper, 50000t/a toluene refining section was designed. The main work of the paper was the design of rectifying column. It mainly included material calculation, heat calculation, theoretical calculation of technological dimension, and calculated specific operating parameters and structure parameters, obtained the bubble point temperature, theoretical plate number, the actual plate number and the minimum reflux ratio and other information. The diameter of the rectifying tower is 2.2m, the height of the tower is 19.2m, the trays of tower are 29 and the distance between neighbouring trays is 0.4m. Secondly, the affiliated equipment was calculated and selected. This included the appropriate top condenser and bottom reboiler. Finally, the process control system was designed based on quality and safe requirements. Key words: Rectification，Toluene，Process Design, Control Settings 目 录 0 绪论………………………………………………………………………………1 1. 设计任务和工作方案………………………………………………………3 1.1 设计任务………………………………………………………………… 3 1.2 设计方案………………………………………………………………… 3 1.2.1 装置流程的确定…………………………