《不同CaCl2浓度对合成纳米CaCO3的影响》-毕业论文（设计）.doc

湖北工业大学毕业设计（论文） PAGE 毕 业 设 计（论文） 题目不同CaCl2浓度对合成纳米CaCO3的影响 姓 名 学 号 0810412103 所在学院 化学与环境工程学院 专业班级 08材料科学与工程一班 指导教师 日 期 2012年5月30日 PAGE I 摘 要 本实验采用碳化法成功制备出了纳米碳酸钙。以氯化钙、氨水和二氧化碳为原料，分别考察了不同氯化钙浓度对合成纳米碳酸钙的影响。X射线衍射仪(XRD)和扫描电子显微镜(SEM)分别对所制备产物的粒度分布（表征粒度的仪器是激光粒度分析仪，简称ZPA），晶型和微观形貌进行了表征。粒度分布结果表明，氯化钙液浓度小于15.0wt%时能获得粒度分布均匀纳米碳酸钙产品。XRD结果表明氯化钙溶液浓度加入量会改变样品的晶型。SEM表明不同氯化钙浓度在确定样品的微观形态上发挥了重要作用。通过本实验，可以得出氯化钙溶液在小于15.0wt%时，可制得粒度分布均匀，分散性良好的纳米碳酸钙粒子。 关键词：纳米碳酸钙；碳化法；氯化钙；氨水 Abstract The experiment method of use carbon was successfully out of nanometer calcium carbonate. With calcium chloride and ammonia carbon dioxide as raw materials, the author examines the different concentration of calcium chloride synthesis influence of nanometer calcium carbonate. X-ray diffraction (XRD) and scanning electron microscopy (SEM), the product was particle size distribution, crystal and microstructure characterization. The results show that particle size distribution, calcium chloride liquid concentration of less than 15.0 wt % can get when uniform distributed particle size of nano CaCO3 products. XRD results show that calcium chloride solution concentration addition amount will change sample of crystal. SEM show that different concentration in the determination of calcium chloride samples on the microstructure of has played an important role. Through the experiment, calcium chloride solution can be obtained in less than 15.0 wt %, made uniform particle size distribution, good dispersion of nano CaCO3 particle. Keywords: Nanometer calcium carbonate; Carbonization method; Carbonization complete; Calcium chloride 目 录 TOC \o 1-3 \h \z \u HYPERLINK \l _Toc326331256 摘 要 PAGEREF _Toc326331256 \h I HYPERLINK \l _Toc326331257 Abstract PAGEREF _Toc326331257 \h II HYPERLINK \l _Toc326331258 绪 论 PAGEREF _Toc326331258 \h 1 HYPERLINK \l _Toc326331259 第一章 文献综述 PAGEREF _Toc326331259 \h 3 HYPERLI