边界热损失对TPS平板法测量物质热导率的影响-中国测试.PDFVIP

第44卷第4期 中国测试 Vol.44 No.4 2018年4月 CHINA MEASUREMENT TEST April袁2018 doi院10.11857/j.issn.1674-5124.2018.04.024 边界热损失对TPS平板法测量物质热导率的影响 张国靖袁 李艳宁 渊天津大学精密仪器与光电子工程学院袁天津 300072冤 摘 要院假想热源法是基于瞬态平面热源渊transient plane source袁TPS冤法测量平板样品导热系数的理论基础袁但是其 没有考虑测量过程中背景材料本身的有限热阻所导致的边界热损失袁从而直接影响导热系数的测量精度遥该文基于 假想热源法和热探测深度理论袁建立一种可实现边界热损失补偿的数学模型遥 该数学模型揭示探头尺寸尧样品厚度 以及背景材料的导热系数和热扩散率对边界热损失的影响遥为验证该数学模型的有效性袁通过变换背景材料和探头 尺寸对不锈钢尧铅尧45钢尧Q235A.F钢尧黄铜尧6061铝合金尧纯铝以及紫铜的导热系数进行测量遥 结果表明院该数学模 型能够对不同的探头尺寸尧平板样品以及背景材料进行有效的热损失补偿袁使导热系数的测量误差从热损失补偿前 的2.14%~3.49%减小到补偿后的-1.39%~0.80%袁显著提高平板样品导热系数的测量精度遥 关键词院导热系数曰瞬态平面热源法曰边界热损失曰假想热源法曰热探测深度 文献标志码院A 文章编号院1674-5124渊2018冤04-0130-07 Effect of boundary heat loss on thermal conductivity measurement with TPS slab method ZHANG Guojing袁 LI Yanning 渊School of Precision Instrument Opto-Electronics Engineering袁Tianjin University袁Tianjin 300072袁China冤 Abstract: Image source method is the theoretical basis for measurement of the thermal conductivity of slab samples based on the transient plane source 渊TPS冤 method. However袁 this theory neglects the boundary heat loss caused by the limited thermal resistance of the background materials during measurement袁 which directly influences the measurement accuracy of the thermal conductivity. Based on image source method and thermal probing depth theory袁 a mathematical model which could effectively compensate the boundary heat loss was built. The model revealed the influence of probe size袁 sample thickness and thermal conductivity and thermal diffusivity of background materials on boundary heat loss. In order to verif