材料分析方法李晓娜6x射线衍射方向.pptxVIP

2.0 引言;2;3;4;5;劳厄实验（1912）;衍射的概念;晶体和X射线的衍射;;10;11;12;13;由劳厄方程推导Bragg方程 ;15;反射条件： I k– k0 I = I K I = 1/dHKL = 2 sinq/l， 得Bragg方程 l = 2 d sinq;“衍射”与“反射”;18;19;20;21;22;23;24;25;26;27;28;周转晶体法的衍射花样 （NaCl单晶，铜靶。35千伏，18毫安，爆光1小时）;30;31;32;33;A powder composed from 4 single crystals in random orientation (left) and the corresponding diffraction pattern (middle). The individual diffraction patterns plotted in the same color as the corresponding crystal start to add up to rings of reflections. With just four reflection its difficult though to recognize the rings.;The right image shows a diffraction pat