《四丁基溴化铵结晶母液合成三丁胺的合成研究》-毕业论文设计（学术）.docVIP

学年论文 × 四丁基溴化铵结晶母液合成三丁胺的合成研究 × 专 业 制药工程学 学生姓名 陈金露 班 级 B制药101 学 号 1010309125 指导教师 蔡照胜 完成日期 2013年06月05号 PAGE ii PAGE I × 四丁基溴化铵的合成研究 × 摘 要：主要说了四丁基溴化铵的合成，合成方法，以及合成后得到的残留的结晶母液的研究，用这个结晶母液制取溴化钙还有三丁胺，以达到废物利用的功效，产业多元化。 关键词：四丁基溴化铵；溴化钙；裂解；浓缩；结晶。 × Tetrabutylammonium bromide Synthesis ofAbstract: The tetrabutylammonium bromide said synthesis, synthesis method, and the resulting residue after the synthesis of the crystallization mother liquor of the study with the crystallization mother liquor from the system and tributylamine calcium bromide, to achieve the effect of the use of waste, industrial diversification. PAGE i 目 录 第一章 文献综述 ···········································································1 1.1 四丁基溴化铵的物理化学性质 ···············································1 1.2 制备四丁基溴化铵的方法 ····················································1 1.3四丁基溴化铵的应用 ·································································2 1.4四丁基溴化铵的生产状况及市场前景 ··································· 2 1.5从四丁基溴化铵结晶母液中的制备三丁胺的方法······················2 1.6 本课题的意义 ··································································2 第二章 实验部分············································································3 2.1 主要试剂及仪器··········································································3 2.2 从结晶母液中制备三丁胺和溴化钙的实验步骤 ·······················3 2.3 从实验中找出最佳催化剂的量 ···························4 第三章 实验结果与讨论 ··························································· 3.1 四丁基溴化铵结晶母液经一系列反应后所得产物量 ······ 3.2 四丁基溴化铵在怎样温度下反应剧烈 ·························· 3.3 实验结论··································································· 致谢 ·······································································································4 葡醛内酯的合成研究 盐城工学院本科毕业论文（ CREATEDATE \@ yyyy \* MERGEFORMAT 2007） —PAGE 6— —PAGE 1— 第一章 文献综述 1.1四丁基溴化铵的物理化学性质 ? 1.2 制备溴化钙的