《用响应面法优化在微波辐射下壳聚糖降解性能的研究》-毕业论文设计（学术）.docVIP

PAGE l 2013届本科毕业论文 论文题目 用响应面法优化在微波辐射下壳聚糖降解性能的研究 学生姓名：******* 所在学院：食 品 学 院 所学专业：食 品 科 学 与 工 程 导师姓名：********* 完成时间：2013年5月 摘要 采用微波辐射技术对壳聚糖进行了降解, 考察了微波辐射功率、辐射时间和降解时的pH 值等因素对低相对分子质量壳聚糖制备的影响。结果表明, 壳聚糖在pH 值7.6, 微波功率为528W ( 中火) , 微波辐射1. 5h 时, 可降解得到相对分子质量小于3000 的低聚壳聚糖,且重复性较好。 关键词: 微波辐射，低聚壳聚糖， 脱乙酰度 STUDY ON THE DEGRADABILITY OF CHITOSAN UNDER MICROWAVE IRRADIATION ************ Abstract The degradability of chitosan was studied under micro wave irradiation. The factors, such as the micro wave irradiating power, the irradiating time, and the pH, would influence the preparation of low-molecular weight chitosan. The results show that chitosan can be degraded into low-molecular weight chitosan which is less than 3000 under the condition that the pH was 7.6, the micro wav e irradiating power w as about 528W, and the irradiating time was 1.5 hours. The product possessed good property of repetition。 Key words: micro wave irradiation，low-molecular weight chitosan;，the degree of deacetylation 目录 TOC \o 1-3 \h \z \u HYPERLINK \l _Toc357004071 引言 PAGEREF _Toc357004071 \h 1 HYPERLINK \l _Toc357004072 1 实验部分 PAGEREF _Toc357004072 \h 2 HYPERLINK \l _Toc357004073 1. 1 实验仪器及药品 PAGEREF _Toc357004073 \h 2 HYPERLINK \l _Toc357004074 1. 2 实验方法 PAGEREF _Toc357004074 \h 2 HYPERLINK \l _Toc357004075 1. 2. 1 壳聚糖溶液的制备 PAGEREF _Toc357004075 \h 2 HYPERLINK \l _Toc357004076 1. 2. 2 壳聚糖的微波降解 PAGEREF _Toc357004076 \h 2 HYPERLINK \l _Toc357004077 1. 2. 3 脱乙酰度的测定 PAGEREF _Toc357004077 \h 2 HYPERLINK \l _Toc357004078 1. 2. 4 相对分子质量的测定[7] PAGEREF _Toc357004078 \h 3 HYPERLINK \l _Toc357004079 1. 2. 5 响应面分析因素水平的选取 PAGEREF _Toc357004079 \h 3 HYPERLINK \l _Toc357004080 1.2 结果与分析 PAGEREF _Toc357004080 \h 3 HYPERLINK \l _Toc357004081 2 结果与讨论 PAGEREF _Toc357004081 \h 6 HYPERLINK \l _Toc357004082 2. 1 辐射功率对壳聚糖降解性能的影响 PAGEREF _Toc357004082 \h 6 HYPERLINK \l _Toc357004083 2. 2 辐射时间对壳聚糖降解性能的影响 PAGEREF _Toc357004083 \h 6 HYPERLINK \l _Toc357004084 2