泡沫镍填料旋转填充床义传质性能研究-化学工程与技术专业毕业论文.docxVIP

北京化工大学硕士学位论文体积传质系数随旋转填充床转速、液体流量和气体流量的增大而增大。相 北京化工大学硕士学位论文 体积传质系数随旋转填充床转速、液体流量和气体流量的增大而增大。相 同条件下，改性后泡沫镍填料旋转填充床比改性前泡沫镍填料旋转填充床 气相体积传质系数平均提高约7％。通过改性前后泡沫镍填料对液膜和气 膜控制体系传质系数强化作用的比较可知，泡沫镍填料旋转填充床对于由 液膜控制的传质过程表现出更加显著的强化效果。进一步对所获得的传质 数据进行各传质系数的关联式拟合，发现各传质系数的理论值与实验值吻 合性较好，偏差维持在±15％之间。 (3)为进一步探究改性填料的传质强化原因，采用自行研制的可视化 平台，研究改性前后填料对液体的切割分散作用。静态可视化研究结果表 明，改性后泡沫镍填料对液滴具有更好的分散性。穿过改性后泡沫镍填料 而分散的液滴直径比未改性的填料减小约20％；在动态可视化实验中，穿 过改性后泡沫镍填料的液滴直径比未改性的平均减小约13％。动态可视化 实验表明，液滴平均直径随填料厚度和旋转填充床的转速的增大而减小。 但是，当液体流量增大时，液滴平均直径随之增大。 关键词：旋转填充床，传质，泡沫镍填料，可视化 万方数据 MLASS MLASS TEANSFER PERFORMANCE OF A ROTATING PACKED BED WITH NICKEL FOAM PACl(ING ABSTRACT As one of the breakthrough technology to strengthen the process，gravity technology has been applied widely to industrial applications．Rotating packed bed isIS thethe core equipment andand paclong 1S an important)ortant parttrt of。。OI tile rotating packed bed，whith is the main place mixing and mass transfer occurred． Selection the type and structure optimization of packing is one of the main measures to improve the mass transfer efficiency．More attention are paied on the optimizing internal components to improve the energy efficiency of rotating packed bed．Therefore，study on mass transfer performance of rotating packed bed with new packing is of great significance． This work modified hydrophobicly the nickel foam packing and charactered．The mass transfer efficiency of the rotating packed bed with modified and non．modified nickel foam packing were examined．Based on the t 6ments． empirical correlationsCorrelatlons on parametersmeters were proposea the possible mechanism for the enhancement of the mass transfer in the IIl 万方数据 万方数据 万方数据 北京化工大学硕士学位论文rotating 北京化工大学硕士学位论文 rotating packed bed with modified nickel foam packing was also explored by a flow visualization method．The main findings are listed below： (1)After the modification of nickel foam packing，the contact angle of the packing is increased by 250．It can be seen that spheres covered with micro-nano-leve