试验材料及方法.doc

杨苏冰，等：原位观察电子束辐照条件下SUS316L钢中辐照肿胀行为 原位观察电子束辐照条件下SUS316L钢中辐照肿胀行为收稿日期：2016-11-22 收稿日期：2016-11-22 项目基金：国家自然科学基金资助项目；2014年钢铁冶金新技术国家重点实验室开放基金资助项目(KF14-03)；中央高校基本科研业务费 通讯作者：杨占兵（1977-），男，博士，副教授，主要从事高能粒子辐照条件下金属晶体中的非平衡现象及其动力学过程方面的研究，E-mail: yangzhanbing@. 杨苏冰1,2，杨占兵1,2，王会1,2，赵世强2 (1.北京科技大学冶金与生态工程学院，北京100083；2.北京科技大学钢铁冶金新技术国家重点实验室，北京100083) 摘 要：辐照诱导的过饱和空位聚集形成空洞，进而引起的奥氏体不锈钢辐照肿胀现象会造成核反应堆内结构材料失效，危害反应堆安全。本文利用超高压电子显微镜，在300~500 ℃区间内，对SUS316L奥氏体不锈钢进行电子束辐照，原位观察辐照过程中空洞演变；辐照结束后，在透射电镜下观察空洞分布，并对空洞尺寸进行测量统计；对比研究了不同温度下空洞演变的差异。结果表明：不同温度时电子辐照30 min后，可观察到点缺陷簇、位错环和空洞。其中450 ℃和500 ℃时，空洞尺寸最大，分别约为13.3 nm和14.5 nm。这是因为辐照温度升高会提高空位扩散能力，最终增大空洞尺寸。本研究结果为预测不同工作温度下奥氏体不锈钢中辐照肿胀提供了实验依据。 关键词：电子束辐照；原位观察；过饱和空位；空洞；辐照肿胀 中图分类号：TL341 文献标志码：A In-situ observation the void swelling behavior in SUS316L steel under electron irradiation YANG Subing1,2, YANG Zhanbing1,2, WANG Hui1,2, ZHAO Shiqiang (1. School of Metallurgical and Ecological Engineering, University of Science and Technology Beijing, Beijing 100083, China; 2. State Key Laboratory of Advanced Metallurgy, University of Science and Technology Beijing, Beijing 100083, China) Abstract: Void swelling in austenitic stainless steel degrades the properties of materials used in reactors due to the accumulation behavior of radiation-introduced excess vacancies, which brings a serious threat to the safety of reactor. In this paper, electron beam irradiations were conducted by high voltage electron microscope in a temperatures range of 300~500 ℃, and in-situ observation of the void evolution was carried out during irradiations. Void distributions were observed and void sizes were measured using transmission electron microscope after irradiations. The difference among the void evolution under different irradiation temperatures were investigated. The results show that large amounts of point defect clusters, loops, and voids form under all electron beam irradiations. In temperature range of 300~500 ℃, void occurs due to the excess vacancies under electron beam ir