烟台成品及散装食用油中塑化剂含量的调查.pdf

7 10 Vol. 7 No. 10 2016 10 Journal of Food Safety and Quality Oct. , 2016 王 颖, 刘海韵, 张桂芳, 王志昱, 张晓瑜, 孙兆鹏* (, 264003) 摘 要: 目的 方法 GB/T 21911-2008, : (1:1, V:V), , 结果 , , (2-) (DEHP)70%(DBP)60%(DIBP)45%(DINP)20%, DEHP 35.7%, DBP 58.3% 结论 , 关键词: ; -; ; Determination of plasticizers in finished and bulk oil in Yantai * WANG Ying, LIU Hai-Yun, ZHANG Gui-Fang, WANG Zhi-Yu, ZHANG Xiao-Yu, SUN Zhao-Peng (Yantai Center for Disease Control and Prevention, Yantai 264003, China) ABSTRACT: Objective To investigate the migration of plasticizers from plastic packaging into finished and bulk oil in Yantai. Methods According to GB/T 21911-2008, the samples were extracted with ethyl acetate: cyclohexane (1:1, V:V), and purified with gel permeation chromatography. Gas chromatography-tandem mass spectrometry (GC-MS/MS) was used for qualitative and quantitative analysis. Results There were low detection rates of plasticizers in finished oils, but high rates in bulk oils. The detection rates of bis(2-ethylhexyl) phthalate (DEHP), dibutyl phthalate (DBP), diisobutyl phthalate (DIBP) and diisononyl phthalate (DINP) were 70%, 60%, 45% and 20%, respectively, and the exceeding rates of DEHP and DBP were respectively 35.7% and 58.3%. Conclusion The finished oil should be chosen when shopping, and bulk oil should not be stored in the non-food-grade plastic b