鱼体中挥发酚的提取与残留分析.PDFVIP

业环境科学学报 园园8熏 7穴2雪:801-804 允燥怎则灶葬造 燥枣 粤早则燥鄄耘灶增蚤则燥灶皂藻灶贼 杂糟蚤藻灶糟藻 鱼体中挥发酚的提取与残留分析 战培荣袁王海涛袁 陈中祥袁卢 玲袁刘 伟 渊中国水产科学研究院黑龙江水产研究所袁农业部渔业环境及水产品质量监督检验测试中心袁黑龙江 哈尔滨 150070 ) 要院挥发酚是重要的环境污染物袁食用被挥发酚污染的鱼损害人体健康袁因此鱼体中挥发酚残留量的准确分析方法研究非常 重要遥本文比较了两种蒸馏方法提取鱼体中挥发酚的效果袁研究了鱼体中挥发酚残留量的测定方法遥结果表明袁水蒸汽蒸馏提取法 效果好袁4-AAP 法适用于处理后样品的分析测定遥 本研究建立的方法袁线性范围0.005耀6.0 mg 窑L-1 袁回收率85.5%耀105% 袁相对标准 偏差 1.6%耀6.3% 袁检出限0.05 mg 窑kg-1 遥 方法实用袁便于操作袁已应用于鱼体中挥发酚残留量的测定遥 ： ；残留 关键词 鱼；挥发酚；水蒸汽蒸馏；提取 中图分类号院X830.2 文献标识码院粤 文章编号院1672-2043(2008)02-0801-04 Extraction and Residue Analysis of Volatile Phenols in Fish ZHAN Pei-rong, WANG Hai-tao, CHEN Zhong-xiang, LU Ling, LIU Wei 渊Heilongjiang River Fisheries Research Institute 袁Chinese Academy of Fisheries Sciences, Fishery Environment and Aquatic Product Quality Supervision Testing Center, the Ministry of Agriculture, Harbin 150070 袁China 冤 Abstract:The volatile phenols are important environment pollutants. The analysis method of volatile phenols residue in fish is very important since eating polluted fish harms to the health of people. The effect of two distillation methods in extracting the volatile phenols residue in fish was compared, and the determination method of volatile phenols residue in fish was studied. The results showed that the steam distillation extraction method was more effective, and 4-aminoantipyrine (4-AAP) method was suitable for the analysis and determination of samples af原 ter treated. The linear range of the method was 0.005~6.0 mg 窑L-1, with relative standard deviations 1.6%~6.3%, the recovery 85.5%~105% and detection limit of 0.05 mg 窑kg-1. The method is practical and simple and has been applied successfully to the determination of volatile phenols in fish. Keywords: fish; volatile phenols; steam distillation; extraction; residue 、石油、制药等行业，其 。 挥发酚主要来源于炼焦 废 国际公认的针对多组分酚类化合物测定的方法 该方