煮绵废水中丝胶粉末的提取及其水溶性研究.PDFVIP

Vol.49 第49卷 No.04, Apr. 2012 2012年04月 第04期 研究与技术 煮绵废水中丝胶粉末的提取及其水溶性研究 卢 霞，胡征宇，匡立岭，陈 启 (苏州大学 纺织与服装工程学院，江苏 苏州 215021) 摘要：利用盐酸酸析法探讨了煮绵废水中丝胶粉末的提取，并研究了其水溶性。对丝胶原液、酸析沉淀后的上清液及丝胶粉末的微 观结构扫描电镜，观察表明：丝胶颗粒并非球形，存在各种形态；干燥后的丝胶粉末由许多微小颗粒聚集而成，且不同的干燥方法 对丝胶粉末的水溶性有影响。 关键词：煮绵废水；丝胶粉末；水溶性；喷雾干燥；扫描电镜；酸析法 中图分类号：TS149 文献标志码：A 文章编号：1001-7003(2012)04-0005-05 Extraction and water-solubility research of sericin powders from the waste water of floss silkworm cooking LU Xia, HU zheng-yu, KUANG Li-ling, CHEN Qi (College of Textile and Clothing Engineering, Soochow University, Suzhou 215021, China) Abstract: The extraction and water-solubility research of sericin powders from the waste water of the floss silkworm cooking were discussed with the hydrochloric acid titration method. The SEM observation of the microstructure of the supernatant and the sericin powders after the deposition of the original sericin solution and the hydrochloric acid titration showed that the sericin powder existed in various kinds of forms but not just the spherical form; the sericin powder after drying is formed by the aggregation of many small particles, and different drying methods have obvious effects on the water-solubility of the sericin powder. Key Words: Waste water of floss silkworm cooking; Sericin powder; Water-solubility; Spray drying; SEM; Acid titration method ) ( 蚕丝是一种极为重要的天然蛋白质纤维，主要由 司，分析纯 ，无水碳酸钠 中国上海试剂总厂，分析 70 % 80 % 20 % 30 % ) (