微波真空辐射制备CuCISi02－Ti02催化剂研究-ResearchGate.PDFVIP

See discussions, stats, and author profiles for this publication at: /publication/296354368 Study on preparation of CuCl/SiO2-TiO2 catalysts under microwave irradiation in a vacuum Article · October 2008 CITATIONS READS 0 151 5 authors, including: Jun Ren Fanhui Meng Taiyuan University of Technology Taiyuan University of Technology 65 PUBLICATIONS   521 CITATIONS    34 PUBLICATIONS    177 CITATIONS    SEE PROFILE SEE PROFILE Some of the authors of this publication are also working on these related projects: Theoretical study of hetergeneous catalysis View project Microwave-assisted preparation of heterogeneous catalysts View project All content following this page was uploaded by Jun Ren on 15 December 2016. The user has requested enhancement of the downloaded file. 第30卷增2 压电与声光 Suppl．No．2 2008年10月 PIEZOELECTECTRICSACOUSTOOPTICS0Ct．2008 文章编号：1004—2474(2008)S2—0121。02 任 军，刘树森，曾 慧，孟凡会，李 忠 (太原理工大学煤科学与技术教育部和山西省重点实验室，山西太原030024) 摘要：采用微波真空辐射法制备一系列CuCl／SiOz—TiO。催化剂，考察了处理温度、时间对CuCl分散及其甲 醇液相氧化羰基化反应活性的影响，比较了微波辐射法(MW)与传统电炉加热(EF)制备的催化剂活性。研究结果 表明，微波辐射可以使CuCl在低温下快速在Si02-TiOz表面形成单层分散，得到的催化剂样品的反应活性也明显 高于电炉加热制备的催化剂。 关键词：微波辐射f真空；氧化羰基化；碳酸二甲酯，单层分散 中图分类号：TN384 文献标识码：A on of underMicrowave CuCI／Si02-TiOz StudyPreparation Catalysts I