固相萃取净化-气相色谱法检测人乳中持久性有机氯农药.PDFVIP

5 7 Vol. 5 No. 7 2014 7 Journal of Food Safety and Quality Jul. , 2014 - 1 1 1 2* 杨国良 , 陈 启, 蔡明明 , 赖世云 , 任一平 (1. , 310014; 2. , 310051) 摘 要: 目的 , 方法 , , 结果 8 5~200 ng/mL, 0.9955~0.9994, 2.6 μg/kg, 70%~122%, 3.91%~10.77% 结论 , , , , 关键词: ; ; ; ; Detection of persistent organochlorine pesticides in human milk by solid-phase extraction and gas chromatography 1 1 1 1 2* YANG Guo-Liang , CHEN Qi , CAI Ming-Ming , LAI Shi-Yun , REN Yi-Ping (1. Beingmate Baby Child Food Co., Ltd, Hangzhou 310014, China; 2. Zhejiang Provincial Center for Disease Prevention and Control, Hangzhou 310051, China) ABSTRACT: Objective To establish a detection method of organochlorine pesticides in human milk and to analyse their concentration in mature human milk from Beijing, Lanzhou and Hangzhou. Methods Human milk samples were extracted with acetonitrile. After purification and enrichment with acidificated silicone solid phase extraction column, the samples were analyzed by using gas chromatography. Re