线性离子阱静电场轨道阱质谱对化妆品中抗生素类成分的快速筛查和确证.PDF

5 12 Vol. 5 No. 12 2014 12 Journal of Food Safety and Quality Dec. , 2014 1 1* 1 2 1 1 1 王凤美 , 牛增元 , 罗 忻 , 李兆永 , 叶曦雯 , 张鸿伟 , 何京澄 (1. , 266002; 2. , 266061) 摘 要: 目的 -/ (ultra high performance liquid chromatography-linear ion trap/orbitrap high resolution mass spectrometry)方法 , ACQUITY BEH C18 , (5 mmol/L 0.1%)-, , 结果 36 5×10-6(5 ppm), r2 0.994, (limit of detection)10 μg/kg, 54.15%~117.55%, (relative standard deviation) 1.19%~13.25%结论 50 , 关键词: ; ; ; / Screening and confirmation of antibiotics in cosmetics by high performance liquid chromatography-linear ion trap/orbitrap high resolution mass spectrometry 1 1* 1 2 1 WANG Feng-Mei , NIU Zeng-Yuan , LUO Xin , LI Zhao-Yong , YE Xi-Wen , ZHANG Hong-Wei1, HE Jing-Cheng1 (1. Technical Center of Shandong Entry-Exit Inspection and Quarantine Bureau, Qingdao 266002, China; 2. Research Center for Marine Ecology, the First Institute of Oceanography, State Oceanic Administration, Qingdao 266061, China) ABSTRACT: Objective To screen and confirm common antibiotics i