气相色谱法测定饮用水中痕量土臭素和二甲基异冰片-分析测试学报.PDF

26 2 V ol126 N o12 2007 3 FEN X I CESH I XU EBAO ( Journal of Ins trum en tal A naly s s) 267~ 269 1 1 1 2 马晓雁 , 高乃云 , 李青松 , 顾国芬 ( 1. , 200092; 2. , 200092) : - ) ) ) ( geosm n, G SM ) ( 2- m ethy l soborneo,l 2-M IB ) , , 10 m n, 1 200 r /m n, N aC l 20 g, pH 5, G SM 2- M IB 10 ng /L : ; ; ; ; : O 6571 71; P64 1112 : A : 1004 - 4957 ( 2007) 02- 0267 - 03 D eterm nat on o f T race G eosm n and 2-M ethy l soborneol n D r nk ng W ater by G as Chrom atography 1 1 1 2 MA X ao-yan , GAO N a-yun , L I Q ng-song , GU Guo-fen ( 1. S tate K ey L aboratory of Po llut on Contro l and R esource R eu se, Co llege of Env ronm ental Sc ence and Eng neer ng, T ongj U n vers ty, Shangha 200092, Ch na; 2. A na lys s Cente r o f Y angshupu W aterw orks n Shangha, Shangha 200092, Ch na) Ab stract: A m ethod for the detect on o f odorants) ) ) geosm n and 2-m e thyl sobo rneo l n dr nk ng w a- terw th l qu d- l qu d m croex trat on by gas chrom atography w as deve loped. T he extract on w as carr ed out n a so lut on of pH 5 w th a dosage of 20 g N aC.l T he optm um st rr ng tm e and rate w ere 10 m n and 1 200 r/m n, respect vely. The l near ranges of the ca l brat on curves fo r GSM and 2-M IB w ere 5- 1 000 ng /L. T