锦纶6聚合切片生产工艺设计说明书.doc

word文档整理分享 参考资料 ` 毕业设计说明书 题 目: 锦纶6聚合切片生产工艺设计 所属系、部 : 材 料 与 环 保 学 院 年级、 专业: 高分子材料加工技术 姓 名: 学 号: 指 导 教 师: 完 成 时 间: [摘要]锦纶-6是合成纤维的第二大化纤，所以不管是在民用还是在工业用上都占着具足轻重的地位。生产锦纶-6的工厂有很多家，所以锦纶-6切片生产工艺是我们作为一个学习化纤工艺的学生必须要研究的课题，本设计使用己内酰胺为原料，采用瑞士伊文达的连续聚合技术（加压预聚合+常压聚合）。利用瑞士进口的聚合VK管，前聚主要是开环和加成反应，后聚主要是部分加成和缩聚反应，前聚吸热反应采用气相联苯加热，后聚放热反应采用液相联苯带走热量。前聚合器可以使单体在过量水分和加热下生成足够多的带氨基和羧基的活性分子，增加在后聚合器的聚合速度，尽量提高单体在前聚合器的转化率，转化率越高，则切片中单体含量越少。采用热水连续萃取工艺，即切片从萃取塔上部进人，由上至下运动，热水由萃取塔底部进入，由下至上与切片逆向运动，萃取掉PA6切片中的单体和低聚物，使切片中可萃取物含量的百分比低于0．5(高速纺)。切片使用热氮气循环干燥，干燥设备基本分为干燥塔和切片冷却器，干燥介质为纯热氮气。本设计的重点在于切片工艺流程说明、工艺原理及参数确定和工艺设备说明，附带介绍原材料的来源和规格和成品质量指标。 Summary Polyamide fibre- 6 is third big chemical fiber of diamars, therefore disregarding the position being degree of seriousness in civil it is more enough to be taking up an utensil on the industrial. 6s factories producing polyamide fibre at present- have many families, therefore polyamide fibre- 6 section productive technologies are problem we must need to study as being a student who studies the chemical fiber handicrafts. Self owns lactam designing usage originally is raw material , the continuous polymerization technology (compression adopt the Germany Zimmer company gets together + in advance ordinary pressure gets together). Use two polymerization VK tubes that Germany entrance, getting together in the front is a ring opening and addition reaction mainly , that the queen gets together is part addition and condensation polymerization reaction mainly , gather endothermic reaction in the front adopt the gas appearance biphenyl to heat, the queen gathers exothermic reaction adopt liquid to look at and appraise a biphenyl taking away quantity of heat. Former polymerization implement can make a monomer generate the activity molecule being enough to bring amidocyanogen and the carboxyl along muchly under bellyful