气相色谱-质谱法测定奶粉及奶制品中的三聚氰胺-分析测试学报.PDF

27 10 V ol127 N o1 10 2008 10 FEN X I CESH I XU EBAO ( Journal of Ins trum en tal A naly s s) 1044~ 1048 - 吴惠勤, 黄 芳, 林晓珊, 邓 欣, 马叶芬, 黄晓兰, 朱志鑫, 罗辉泰 ( , 510070) : - ( GC - M S) , ( S IM ) , DB- 1 M S , 280 e , 75 e , 1 m n, 30 e /m n 290 e H e, 110 mL /m nEI , m / z 171 285327342 SIM , 4 , m /z 327 010 1~ 50 m g / L, 90% ~ 98% , 1 L g / kg, 5 L g / kg 2, , , , , , : ; ; ; - ; : O 657163; TS2521 51 : A : 1004 - 4957 ( 2008) 10 - 1044 - 05 D eterm nat on ofM elam ne n M lk Pow der and M lk Products by G as Chrom atography- M ass Spectrom etry WU H u -q n, HUANG F ang, L IN X ao-shan, DENG X n, MA Y e-fen, HUAN G X ao- lan, ZHU Zh -x n, LUO H u -ta ( Guangdong K ey Laboratory of Chem ca l Em ergency, Ch na N at onal A nalyt cal C enter( G uangzhou) , Guangzhou 510070, Ch na) Abstract: A new m ethod fo r determ nat on of m elam ne n m lk pow der and m lk products by gas chrom atography - m ass spectrum w th se lected on m on to r( GC- MS /SIM ) w as establ shed n th s pa- per. T he cond t ons for GC - M S w ere optm zed, and the ons se lected w ere m /z 171, 285, 327, 342. Qual tat ve assessm ent w as