气相色谱法测定生物柴油样品中脂肪酸甲酯和脂肪酸甘油酯的含量.PDF

24 5 Vol. 24 No. 5 20059 FENXI CESHI XUEBA (Journal of Instrumental Analysis) 66~ 68 1 2 1 李长秀 , 唐 忠 , 杨海鹰 ( 1. , 100083; 2. , 210033) : , , , , , : ; ; : 657. 71 : A : 1004- 4957( 2005) 05- 0066- 03 Determination of Fatty Acid Methyl Esters and Glycerides in Bio_diesel Sam les b GC p y 1 2 1 LI Chan _xiu, TANG Zhon , YANGHai_ in g g y g ( 1. Research Institute of Petroleum Processin , SIN PEC, Bei in 100083, China; g j g 2. Jinlin Com an , SIN PEC, Nanin 210033, China) g p y j g Abstract: Agaschromatographicmethodisdevelopedfor the determinationoffattyacidmethylesters andglyc- erides in bio_diesel sam les. A non_ olar ca illar column ofhi h tem erature tolerance was used for se ara- p p p y g p p tion. The sam le was introduced viathe cool on_column inector and detected b theflame ionization detector p j y without pre_derivation. The internal standard method was used for quantification. The method is simple and ra id and can be used for the determination of the conversion rate of fatt acid l cerides in the re aration p y gy p p process of bio_diesel. Ke words: Bio_diesels; Fatt acid l cerides; Gas chromato ra h y y gy g p y , , , , ( C16~ C22) , , ,