响应面优化超声辅助花蛤壳丙酸钙制备工艺研究.PDFVIP

第40 卷第1 期 Vol.40 No.1 井冈山大学学报( 自然科学版) 2019 年1 月 Jan. 2019 Journal of Jinggangshan University (Natural Science) 13 井冈山大学学报( 自然科学版) 13 文章编号：1674-8085(20 19)01-00 13-06 响应面优化超声辅助花蛤壳丙酸钙的制备工艺研究 林 洵 (漳州职业技术学院食品工程学院，福建，漳州 363000) 摘 要：以花蛤壳为原料，采用响应面法对超声辅助花蛤壳丙酸钙的制备工艺进行了优化 在单因素试验的基础 上，以丙酸钙产率为响应值，选取超声时间、超声温度、液固比和酸壳比为自变量，利用Box-Behnken 设计和响 应面法对各自变量及其交互作用对丙酸钙产率的影响进行了研究，得到了四元二 多项式回归方程模型 超声辅 助制备花蛤壳丙酸钙的最佳工艺条件为：超声时间120 min 、超声温度71℃、液固比18.3 mL/g 和酸壳比1.8 mL/g ， 在此条件下测得丙酸钙产率为93.95%，与预测值 （94.07% ）相比，其相对误差为0.13%，说明响应面优化超声辅 助制备花蛤壳丙酸钙的工艺参数具有较高的准确性和有效性，该方法可用于花蛤壳丙酸钙制备工艺的优化 关键词：花蛤壳；丙酸钙；制备；优化 中图分类号：TS202/O69 文献标识码：A DOI:10.3969/j.issn.1674-8085.20 19.01.004 OPTIMIZATION OF ULTRASONIC-ASSISTED PREPARATION OF CALCIUM PROPIONATE FROM CLAM SHELLS BY RESPONSE SURFACE METHODOLOGY LIN Xun (School of Food Engineering, Zhangzhou Institute of Technology, Zhangzhou, Fuj ian 363000, China) Abstract: The preparation process of ultrasonic-assisted clam shells calcium propionate was optimized using the response surface methodology. On the basis of single factor experiment, setting the factors the ultrasonic time, ultrasonic temperature, liquid-solid ratio and acid-shell ratio as independent variables, the calcium propionate yield as the response value, the effects of the factors and their interaction on the yield of calcium propionate were studied by the Box-Behnken design and response surface methodology, and a quadratic quadratic polynomial regression equation model was obtained. The optimum conditions for the preparation proces