原创力文档- 1、原创力文档（book118）网站文档一经付费（服务费），不意味着购买了该文档的版权，仅供个人/单位学习、研究之用，不得用于商业用途，未经授权，严禁复制、发行、汇编、翻译或者网络传播等，侵权必究。。
- 2、本站所有内容均由合作方或网友上传，本站不对文档的完整性、权威性及其观点立场正确性做任何保证或承诺！文档内容仅供研究参考，付费前请自行鉴别。如您付费，意味着您自己接受本站规则且自行承担风险，本站不退款、不进行额外附加服务；查看《如何避免下载的几个坑》。如果您已付费下载过本站文档，您可以点击 这里二次下载。
- 3、如文档侵犯商业秘密、侵犯著作权、侵犯人身权等，请点击“版权申诉”（推荐），也可以打举报电话：400-050-0827(电话支持时间：9:00-18:30)。
查看更多
26 5 Vol. 26, No. 5
2006 5 Acta Scientiae Circumstantiae M ay, 2006
, , . 2006. [J]. , 26( 5): 865- 869
Zheng J, ChenM J, Zhang B. 2006. Preparation of ammonium iron blue from pyrite cinders andwasted ammonium sulfate solution [ J]. A cta Scientiae
C ircumstantiae, 26( 5): 865- 869
*
郑雅杰 , 陈梦君, 张 宝
中南大学冶金科学与工程学院, 长沙 410083
: : :
: , ,
- 1
0. 346 0. 173mo l L . 1. 15!1, 0. 200 mo l
- 1
L , 80 ∀ 10m in. 100∀ 1 h, 50% 2 h, 70
∀ 10% 3 h..
GB 186088 HG/T. SEM , 20 nm; XRD ,
Fe [ Fe( CN) ] .
4 6 3
: ; ; ; ;
: 2006) : X781. 3 : A
Preparation of ammonium iron blue from pyrite cinders and wasted ammonium
sulfate solution
*
ZHENG ajie , CHENM engjun, ZHANG Bao
College ofM etallurgical Science and Engineering, CentralSouthU niversity, Changsha410083
Received 17 June2005; received in revised form 13M arch 2006; accepted 23 March 2006
Abstract: Copperas prepared from pyrite cinderswas put into purified waste ammonium sulfate solution from iron yellow produced by ammoniamethod,
- 1 - 1
and the concentrations of theFeSO and (NH ) SO were0346mo l L and 0. 173mo l L . Thewhite slurrywas obtained bymeans that them ixed
4 4 2 4
solution of ferrous sulfate and ammonium sulfate ( themole ratio was 1. 15!1) was added into 0. 200 mo l L- 1 sodium ferrocyanide solution, and the
reacting temperature had been at 80∀ for 10m ins. Ammonium iron bluewas prepared after thewhite slurry had been boiled at 100 ∀ for 1 h, added
50% sulfuric acid then boiled at 100∀ for2 h, and oxidized at 70 ∀ for 3 h by 10% N aC lO solution. Moreover, the p
文档评论（0）