牛奶中三聚氰胺的表面增强拉曼光谱检测法与国标检测法的比较.PDFVIP

5 10 Vol. 5 No. 10 2014 10 Journal of Food Safety and Quality Oct. , 2014 1 2 1 1* 杨 欣 , 王 军 , 苗 虹 , 周萍萍 (1. , , 100021; 2. , 100124) 摘 要: 目的 (GB/T 22388-2008/ -/ ) 方法 结果 ; 117.3% 13.2%, 106.2% 8.9%结论 , 关键词: ;-/; ; Comparison between surface-enhanced Raman scattering and the national standard method for the detection of melamine in milk 1 2 1 1* YANG Xin , WANG Jun , MIAO Hong , ZHOU Ping-Ping (1. Key Laboratory of Food Safety Risk Assessment of Ministry of Health , China National Center for Food Safety Risk Assessment , Beijing 100021, China; 2. Beijing University of Technology, Beijing 100124, China) ABSTRACT: Objective To compare surface-enhanced Raman scattering (SERS) and the national standard method (GB/T 22388-2008 the 2nd method/liquid chromatography–mass spectrometry/mass spectrometry, LC-MS/MS) for the detection of melamine in milk. Methods Melamine in milk was tested by SERS and the national standard method, respectively. Results SERS was consistent with the national standard method for the positive samples confirmed; the average recovery and RSD of SERS were 117.3% and 13.2%, while the average recovery and RSD of the national standard method were 106.2% and 8.9%, respectively. Conclusion SERS is suitable for the rapid screening test for melamine in milk; the national standard m