离子色谱法检测售常见15种蔬菜中7种单糖和双糖-食品安全质量.pdf

7 1 Vol. 7 No. 1 2016 1 Journal of Food Safety and Quality Jan. , 2016 -15 7 1* 2 1 1 于 丽 , 王 婷 , 周健南 , 钟 钰 (1. , 110016; 2. , 110016) 摘 要: 目的 -(IC-PAD) 方法 , DIONEX CarboPac PA10 , DIONEX CarboPac PA10 , NaOH CH3COONa , , 结果 7 343664 3 μg/L, (0.05~20 mg/L)15 1.48%~6.41%, 7 90%~97%结论 , 关键词: ; ; ; Ultrasonic extraction-ion chromatography detection of 7 kinds of monosaccharides and disaccharides in 15 kinds of common vegetables 1* 2 1 1 YU Li , WANG Ting , ZHOU Jian-Nan , ZHONG Yu (1. Shenyang Entry-Exit Inspection and Quarantine Bureau, Shenyang 110016, China; 2. Vocational and Technical School, Shenyang Pharmaceutical University, Shenyang 110016, China) ABSTRACT: Objective To establish a method for the detection of water-soluble galactose, glucose, xylose, glucose, sucrose, lactose, and maltose in vegetables by ion chromatography - pulse integral amp test (IC-PAD). Methods Water immersion ultrasonic extraction and membrane filtration method were used to treat vegetable samples, DIONEX CarboPac PA10 anion exchange column as the analysis of column, DIONEX CarboPac PA10 as protection column, with the combination of NaOH and CH3COONa solution as mobile phase. Samples wer