第一章样品前处理支撑液液萃取和蛋白质沉淀介绍.pptVIP

Tianjin University 第一章 样品前处理方法专题介绍三：支撑液液萃取、 蛋白质沉淀 一、支撑液液萃取 Solid-supported liquid liquid extraction (SLE) 以传统液液萃取原理为基础，结合固相萃取 支撑体易于相分离的特点，以一种吸附性高、惰性好、比表面积大的多孔填料为介质，从而实现快速和高通量样品制备； 硅藻土-SLE The process of sample analysis by SLE and HPLC First reported in 1997 by Johnson and co-workers SLE has many advantages compared with LLE Simple operation No emulsification High recovery rate 硅藻土-SLE Investigation of packing and filled method Characterization of packing (A) Inert packing treated by high temperature burning and acid cleaning and (B) Detail view of the inert packing A B SLE样品前处