标准、规范、准则_EPA Method 8061A Phthalate Esters by Gas Chromatography with Electron Capture Detection (GC_ECD) - Revision 1.pdf

METHOD 8061A PHTHALATE ESTERS BY GAS CHROMATOGRAPHY WITH ELECTRON CAPTURE DETECTION (GC/ECD) 1.0 SCOPE AND APPLICATION 1.1 Method 8061 is used to determine the identities and concentrations of various phthalate esters in aqueous and solid matrices including groundwater, leachate, soil, sludge and sediment. The following compounds can be determined by this method: ______________________________________________________________________________ Compound Name CAS No.a Benzyl benzoate (Int. Std.) 120-51-4 Bis(2-ethylhexyl) phthalate 117-81-7 Butyl benzyl phthalate 85-68-7 Di-n-butyl phthalate 84-74-2 Diethyl phthalate 84-66-2 Dimethyl phthalate 131-11-3 Di-n-octyl phthalate 117-84-0 ______________________________________________________________________________ a Chemical Abstract Service Registry Number. 1.2 Table 1 lists the method detection limits (MDLs) for the target analytes in a water matrix. The MDLs for the components of a specific sample may differ from those listed in Table 1 because MDLs depend on the nature of interferences in the sample matrix. Table 2 lists the estimated quantitation limits (EQLs) for other matrices. 1.3 The following compounds may also be analyzed by this procedure or may be used as surrogates: Compound Name CAS No.a Bis(2-n-butoxyethyl) phthalate 117-83-9 Bis(2-ethoxyethyl) phthalate 605-54-9 Bis(2-methoxyethyl) phthalate