标准、规范、准则_EPA Method 609 Nitroaromatics and Isophorone.pdf

APPENDIX A TO PART 136 METHODS FOR ORGANIC CHEMICAL ANALYSIS OF MUNICIPAL AND INDUSTRIAL WASTEWATER METHOD 609—NITROAROMATICS AND ISOPHORONE 1. Scope and Application 1.1 This method covers the determination of certain nitroaromatics and isophorone. The following parameters may be determined by this method: Parameter STORET No. CAS No. 2,4-Dinitrotoluene . . . . . . . . . . . . . . . . . . . . . . . . . . . . 34611 121-14-2 2,6-Dinitrotoluene . . . . . . . . . . . . . . . . . . . . . . . . . . . . 34626 606-20-2 Isophorone . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 34408 78-59-1 Nitrobenzene . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 34447 98-95-3 1.2 This is a gas chromatographic (GC) method applicable to the determination of the compounds listed above in municipal and industrial discharges as provided under 40 CFR Part 136.1. When this method is used to analyze unfamiliar samples for any or all of the compounds above, compound identifications should be supported by at least one additional qualitative technique. This method describes analytical conditions for a second gas chromatographic column that can be used to confirm measurements made with the primary column. Method 625 provides gas chromatograph/mass spectrometer (GC/MS) conditions appropriate for the qualitative and quantitative confirmation of results for all of the parameters listed above, using the extract produced by this method. 1 1.3 The method detection limit (MDL, defined in Se