辐射接枝制备质子交换膜实验进展及问题幻灯片.pptx

辐射接枝制备质子交换膜实验进展及问题 2 实验目的 Radiation Graft Membrane Better Cheaper 3 实验内容 4 实验内容 23.54mg 22.40mg 22.59mg 26.70mg 26.85mg 14.72mg 0.8 g in 10ml DMF 6.6325g单体 +15ml 正丙醇 6.7071单体 +15ml 二氧六环 0.82g 单体 +5ml DMF 80℃，48h 80℃，48h 80℃，48h 2 3 1 5 实验内容 实验装置 磁子搅拌 水浴加热 溶剂冷凝回流 Ar气保护 6 实验内容及结果 H2O 1 dry DMF cast by H2O 2 dry DMF cast rinse H2O 3 dry DMF cast Before graft： 68.53mg After graft ：53.60mg Before graft： 68.27mg After graft ：76.70mg GD =12% Before graft： 0.8 g After graft ：0.4127g 7 实验内容及结果 H2O 1 dry DMF cast by H2O 2 dry DMF cast rinse H2O 3 dry DMF cast Alkaline Acid Alkaline Acid Alkalin