无铁污染搅拌球磨法制备高纯超细硅微粉的研究_蒋述兴.pdfVIP

29 1 矿　冶　工　程 Vo.l29 №1 2009 02 MININGANDMETALLRGICALENGINEERING February2009 ① 蒋述兴 (, 54 1004 ) 　:, 。 D, , 1 μm 50 。, 1 μm, 。 :;;;; :TD9 85 :A :0253-6099(2009 )0 1-00 86-04 StudyonthePreparationofHighpurityand ltrafineQuartzMicropowders byAgitationBallMillingMethodwithoutIronContamination JIANGShu-xing (KeyLaboratoryofNewProcessingTechnologyforNonferrousMetalsandMaterial,sMinistryofEducation, Guilin niver- sityofTechnology, Guilin541004, Guangx,iChina) Abstrac:t singyttrium-stabilizedziconiaballsasgrindingmedi,ahighpurityandultrafinequartzmicropowderswere preparedbypulverizingintheagitationmillinwhichthegrindingtubeinteriorandagitatorlinedwiththepolyurethane. ThechangelawofD withthevariationsofgrindingtmieoftheagitationmillwasstudiedandthecontaminationlevelof 50 yttrium-stabilizedzirconiaballsonquartzmicropowderswasinvestigated.Thechemicalcompositionandshapecharacters ofultrafinequartzmicropowdersbelow1 μmwereanalizedanddiscussed.Theexpermientalresultsshowthathighpurity andultrafinequartzmicropowdersbelow1 μmcanbeobtainedbygrindingquartzsandbyagitationmillbutitisdifficult toobtainspericalquartzmicropowders. Keywords:quartzmicropowder;sagitationballmilling;ballmillingmedia;zirconiaballs;withoutironcontamination 　　, , SiO 99.94%, -0.074 mm 2 、、、、、、 3 37.39%;: 6.0 g/cm, 、、。 9, 3 mm;:。 、 ZJM20 T ( 。、。 ), 6 L, :0 ～ 、、、。 1 200 r/min, 0.25 mm;LS-POP ,