硅硼玻璃在可伐合金表面的润湿规律.pdf

80 / 2009 11 Wetting Behavior of Borosilicate Glass on Kovar Alloy 1, 2 1 , ( 1 , 100083; 2 , 518055) 1, 2 1 L O Da-wei , SHEN Zhuo-shen ( 1 School of Materials Science and Engineering, niversity of Science and T echnology Beijing, Beijing 100083, China; 2 School of Applied Chemistry and Biotechnology; Shenzhen Polytechnic,Shenzhen 518055, Guangdong, China) : FeO FeO+ Fe O 1000 3 4 , SEM ,:, FeO FeO+ Fe O 3 4 2523,, , : ; ;; : TG441 : A : 1001-4381(2009) 11-0080-04 Abstract: T he wettability of borosilicate glass on Kovar with oxides of FeO and FeO+ Fe3 O4 respec- tively was studied as a function of holding time at 1000 by the sessile drop method. The contact an- gle and drop diameter were measured by the VHX-100K digital microscopy. T he surface micrographs of halo and cross-sections of glass and kovar were investigated by SEM, and the chemical composition of halos was studied by EDS analysis. Theresults show that the contact angle all decreases as thetime 3 4 increases, and the final contact angles are 25and 23for FeO and FeO+ Fe O , respectively. Two halos are observed in the wetting process. By analyzing the changeof contact angle, halo and drop d-i ameter, wetting process could be divided into three stages: initial period,