bifeo3微晶的水热制备工艺及其磁性研究studyonthepreparationmethodofbifeo3;byhydrothermalmethodanditsmagnetism.pdfVIP

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bifeo3微晶的水热制备工艺及其磁性研究studyonthepreparationmethodofbifeo3;byhydrothermalmethodanditsmagnetism.pdf

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Material Sciences 材料科学, 2011, 1, 107-111 /10.12677/ms.2011.13019 Published Online October 2011 (/journal/ms/) Study on the Preparation Method of BiFeO Crystallite 3 by Hydrothermal Method and Its Magnetism 1 1 2* Qingsheng Liu , Weini Chen , Hongri Liu 1Hubei Mechanical Industrial School, Huangshi 2Hubei Key Laboratory of Pollutant Analysis and Reuse Technology, Hubei Normal University, Huangshi Email: lhr1229@126.com Received: Sep. 28th, 2011; revised: Oct. 8th, 2011; accepted: Oct. 10th, 2011. Abstract: An improved hydrothermal method was adopted to prepare BiFeO crystallite using Bi(NO ) ·5H O, 3 3 3 2 Fe(C H O ) as raw materials and 2-Aminoethanol as alkaline precipitant. The effects of the quantity of pre- 5 7 2 3 cursor precipitate, the concentration of mineralizer, and the reaction temperature on the morphology of prod- ucts, size and structure were studied. The results showed that the size decreases with quantity of precursor precipitate, and increases with reaction temperature. XRD results indicated that pure BiFeO3 can be obtained by the precursor with a concentration lower than 0.005 M reacting at 200˚C. TEM results indicated that the BiFeO3 nanoparticles present prefect mono-domain structure. Analyzing on magnetism showed that the BiFeO3 nanoparticles present weak antiferromagnetic order. Keywords: BiFeO Powder; Hydrothermal Method; Ferromagnetism; Multiferroic 3