XRD射线衍射分析方法.pdfVIP

XRD APPLICATION NOTE Pair distribution function analysis Total scattering experiments using high-energy X-rays on a laboratory system Introduction Recent years have shown an increased Summary interest in the study of nanocrystalline Analyzing powder diffraction data materials due to their specific properties of nanocrystalline and amorphous for application in e.g. semiconductors, materials using the atomic pair pharmaceuticals and polymers. distribution function (PDF) method Structural information about these provides useful information about materials is present as broad, not well the long- and short-range ordering defined features in a diffractogram. of the atoms in the materials. We Analysis of nanomaterials therefore have developed the application requires a total scattering approach, of PDF analysis on a standard including both Bragg peaks and diffuse laboratory system employing an scattering. One of the most promising (a) X-ray tube with either a silver or a analytical methods used is atomic pair molybdenum anode as X-ray source. distribution function (PDF) analysis. Data obtained from a variety of Origi