SANS在高分子材料应用-刘栋.pptxVIP

Recent Applications of SANS-Suanni in Polymeric Materials;Contents;Contents;What SAS measures?;(1) What can SANS do-Chain labeling;(1) Chain labeling-Molecular alignment ;(1) Chain labeling-Polymer crystallization;(1) What can SANS do- contrast matching/variation;(1) Unique features of SANS- Contrast matching ;(1) Unique features of SANS-Contrast variation ;Contents;(2) Chain labeling-crystallization/rheology;(2) Rheo-SANS apparatus;(2) Applications-Flow induced crystallization;(2) Sample preparation;(2) nucleation morphologies and draw ratio;(2) In situ SANS;(2) The microscopic chain deformation;(2) isothermal crystallization;(2) Schematic of motions of chain during FIC;Contents;(3) Background and sample preparation ;;SANS profiles for silica-filled silicone rubber with a series of ΦSi;Fitting-Beaucage model;Dong Liu et al. Composites Science and Technology 165 (2018) 373–379;Contents;(4) Contrast variation SANS on silicone rubber;(4) Contrast variation SANS-Swollen;(4) Partial scattering functions ;(4) Model;(4) Model functions fitted to experimental results;(4) Fitting results;(4) TEM observations;Contents;(5) Contrast matching ;SAXS;(5) Nano-composites in crystalline matrix ;(5) Nano-composites in crystalline matrix ;(5) Nano-composites in crystalline matrix ;41;Conclusion;Further Reading;Funding: NSFC, ICDD, CAEP Beam-time: SSRF, BSRF, NSRL Experts: Prof. L.B. Li (USTC), Prof. Y. Liu (NIST);Thanks for your attention!