分析采样与制样操作 第3章实验练习 实验7-水中溶解氧含量的测定 第3章实验练习 实验7-水中溶解氧含量的测定.pptVIP

Sino-Dutch Demonstration Researcher and Training Centre for Water Treatment Sino-Dutch Demonstration Researcher and Training Centre for Water Treatment Sino-Dutch Demonstration Researcher and Training Centre for Water Treatment Sino-Dutch Demonstration Researcher and Training Centre for Water Treatment Sino-Dutch Demonstration Researcher and Training Centre for Water Treatment Sino-Dutch Demonstration Researcher and Training Centre for Water Treatment Sino-Dutch Demonstration Researcher and Training Centre for Water Treatment Sino-Dutch Demonstration Researcher and Training Centre for Water Treatment Sino-Dutch Demonstration Researcher and Training Centre for Water Treatment Sino-Dutch Demonstration Researcher and Training Centre for Water Treatment Sino-Dutch Demonstration Researcher and Training Centre for Water Treatment Sino-Dutch Demonstration Researcher and Training Centre for Water Treatment 水中溶解氧含量的测定 Sino-Dutch Demonstration Researcher and Training Centre for Water Treatment 一、概 述 1、测定溶解氧的原因： ⑴通过测定DO判断水体是否受到污染 ⑵是活性污泥处理系统的重要监控指标 ⑶为测定BOD5打基础 Sino-Dutch Demonstration Researcher and Training Centre for Water Treatment 2、测定方法的选择 碘量法 修正法碘量法 膜电极法 清洁水可直接采用碘量法测定 Sino-Dutch Demonstration Researcher and Training Centre for Water Treatment 2、测定方法的选择 碘量法 修正法碘量法 膜电极法 叠氮化钠修正法：水样中NO2--N含量0.05mg/L, Fe2＋1mg/L时，适用于多数污水及生化处理出水； 高锰酸钾修正法：水样中Fe2＋1mg/L； 明矾絮凝修正法：水样有色或有悬浮物； 硫酸铜一氨基磺酸絮凝修正法：含有活性污泥悬浊物的水样； Sino-Dutch Demonstration Researcher and Training Centre for Water Treatment 2、测定方法的选择 碘量法 修正法碘量法 膜电极法 根据分子氧透过薄膜的扩散速率来测定水中溶解氧。方法简便、快速，干扰少，可用于现场测定。 Sino-Dutch Demonstration Researcher and Training Centre for Water Treatment 二、试验目的 （1）熟悉碘量法测定水中溶解氧的原理及过程 （2）掌握滴定管的使用 （3）熟练掌握滴定终点的控制 Sino-Dutch Demonstration Researcher and Training Centre for Water Treatment 三、碘量法原理 (白色沉淀) 水样中加入硫酸锰和碱性碘化钾，水中溶解氧将低价锰氧化成高价锰，生产四价锰的氢氧化物沉淀 (棕色沉淀) 加酸后，氢氧化物沉淀溶解并与碘离子反