2016-OPRD-真空干燥机清洗核磁管.pdfVIP

Communication pubs.acs.org/OPRD Vacuum Desiccator as a Simple, Robust, and Inexpensive NMR Tube Cleaner Thanh Binh Nguyen* Institut de Chimie des Substances Naturelles - CNRS-ICSN UPR 2301, Universite Paris-Sud, 1 avenue de la Terrasse, 91198́ Gif-sur-Yvette Cedex, France Scheme 1. NMR Tube Cleaner ABSTRACT: A simple, robust, and inexpensive apparatus for cleaning several NMR tubes is easily fit up and used . ) s. from readily available glassware, including a beaker, a C e T l c desiccator, and a rotary evaporator vacuum pump. i U t ( r a 4 4 d : e 0 h 0 s : i 0 l 1. INTRODUCTION b 1 u t p a 8 e As part of our everyday work on the finding and optimization of r 1 a 0 h new reactions, we were struck by the need for an effective 2 s , y 5 l method to clean rapidly several NMR tubes in a convenient 1 e t r a manner with as little as solvent as possible from readily e m b i o t t i available labware. Commercially available glasswares for this c g e O l purpose are expensive, fragile, solvent consuming, not easy to n o t o V w handle, and more importantly, not suitable for cleaning many I o tubes at once. Solutions for these drawbacks have been