(完整版)化学实验(英文版).docxVIP

Amidation of Carboxylic Acids:preparation of Acetanilide Chen Xiaoling Class2 2012364217 一、 Purpeses and Requirements Learn the principles and operation of aniline aceltylation. Consolidate the recrystallization method and the principle of purflication of organic compounds. 二、 The experimental princinple and devices. Principle Acetanilide can be prepared from aniline in several ways, using acetyl chloride,acetic anhydride or glacial acetic acid as starting materials. Acetyl chloride reacts very vigorously. Acetican hydride is preferred for a laboratory synthesis because its rate of hydrolysis