实验设计——氯化铵的制备.docVIP

实验设计 —— 氯化铵的制备 The Production of NHCl 4 Purposes (1) to master some fundamental operation of performing an experiment. b5E2RGbCAP (2) to confirm the relation of the solubility of salt and temperature. p1EanqFDPw (3) to master the method to determine the percentage yield of nitrogen. DXDiTa9E3d Principles (1) 2NaCl + (NH)SO ? NaSO + 2 NHCl 424244 (2) solubility data NaCl 35.7 35.8 36 36.2 36.5 36.8 37.3 37.6 38.1 38.6 39.2 (NH)SO 70.6 73 75.4 78 81 84.8 88 91.6 95.3 99.2 103.3 424 NaSO?10HO 4.7 9.1 20.4 41 / / / / / / / 242 NaSO / / / 49.7 48.2 46.7 45.2 44.1 43.3 42.7 42.3 24 NHCl 29.7 33.3 3