15万吨丙烯酸精制工艺设计.pdf

ZB 大学 2011 届毕业设计说明书 年产15万吨丙烯酸生产车间汽提、精制工段工艺设计 摘 要 本设计综述了国内外丙烯酸生产的工艺及其发展前景。在对各种丙烯酸的 生产工艺进行详细比较的基础上，选择了丙烯两步氧化生产工艺生产丙烯酸，汽提 和精制工段采用了3塔流程。在物料衡算和热量衡算的基础上，进行了主体设备设 计、辅助设备选型以及车间布置等，完成了年产 15万吨丙烯酸生产车间汽提、精 制工段工艺设计，并绘制了主体设备图、工艺流程图及车间布置图等，对整个工艺 方案进行了经济、环保和安全评价，表明该工艺可行，经济合理。 关键词 丙烯酸，汽提，精制，工艺设计 ZB 大学 2011 届毕业设计说明书 Design of Stripping、Refinin Section for annual output of 150,000 tons acrylic acid technology Abstract The acrylic acid process and its development prospects at home and abroad were summaried in this design. On the base of detailed comparison between various acrylic acid processes, select two-step oxidation of propylene acrylic acid production technology, stripping and refined Section 3 tower process used 。On the base of material balance and heat balance, the main equipment was designed, the style of auxiliary facilities were chosen, the workshop was arranged and the process Design stripping, refinin section for annual output of 150,000 ton acrylic acid technology in the workshop technology design was completed.,besides, the main equipment map, the process flow diagram and the workshop layout and so on were drawn up, and the entire technology program of economic, environmental and safety evaluation shows that the technology is feasible and economically reasonable. Keywords acrylic acid, stripping, refinin, technology design 中北大学 2011 届毕业设计说明书 目 录 1 绪论 1 1.1 丙烯酸概述 1 1.1.1 丙烯酸物化性质 1 1.1.2 丙烯酸用途 1 1.2 国内外丙烯酸产品需求 1 1.2.1 国外需求状况 1 1.2.2 国内需求状况2 2 工艺设计3 2.1 国内外丙烯酸生产工艺概述3 2.1.1 国外生产状况3 2.1.2 国内生产状况4 2.2 反应工段工艺选择4 2.3 后续精制工段工艺对比及选择5 2.3.1 各大公司精制工艺对比5 2.3.2