实验所用的主要仪器如下(译文).docx

Themaininstrumentsusedintheexperimentareasfollows:mufflefurnace,tubefurnace,centrifuge,constanttemperatureoscillator,pHmeter,centrifugetube(10mL,50mL)glassrod,measuringcylinder,pipette(1mL,5mL,10mL),volumetricflask(25mL,50mL,10mL,250mL,500mL,1000mL),quartzmortar,(20mesh,100mesh,200mesh)sieve,syringe,mixedcellulosemicroporousfiltermembrane,electronicanalyticalbalance,conicalflask,beaker,etc.AsshowninTable3-1.

Table3-1Mainexperimentalinstruments

Instrumentandequipmentname

model

Manufacturer

Vacuumtubehigh-temperaturesinteringfurnace

OTF-1200X

HefeiKejingMaterialTechnologyCo.,Ltd

UVvisiblespectrophotometer

UV-5500

ShanghaiYuanxiInstrumentCo.,Ltd

X-rayphotoelectronspectrometer

ThermoKalpha

ThermoFisherScientific(China)TechnologyCo.,Ltd

X-raydiffractometer

BrookeD8ADVANCE

Brooke(Beijing)TechnologyCo.,Ltd

Fouriertransforminfraredspectrometer

NICOLETis10

ThermoFisherScientific(China)TechnologyCo.,Ltd

Specificsurfaceareaandporesizeanalyzer

ASAP2460

Microelectronics,Inc

Fieldemissionscanningelectronmicroscope

NovaNanoSEM450

ThermoFisherScientific(China)TechnologyCo.,Ltd

Elementanalyzer

ElementalVarioMACROcube

ElmontaTrading(Shanghai)Co.,Ltd

ICP-OES

NexION300X

PerkinElmer,USA

Desktopconstanttemperatureoscillator

IS-RDD3

SuzhouJiemeiElectronicsCo.,Ltd

3.3.2Experimentalreagents

Thereagentsusedintheexperimentmainlyincludepotassiumdichromate,ferricchloride,hydrochloricacid,sulfuricacid,hydrofluoricacid,etc.ThespecificreagentspecificationsareshowninTable3-2.

Table3-2Mainexperimentalreagents

name

specifications

Manufacturer

potassiumdichromate

Analyticalpurity

ChinaNationalPharmaceuticalGroupChemicalReagentCo.,Ltd

Ferricchloride

Analyticalpurity

TianjinGuangfuTechnologyDevelopmentCo.,Ltd

sodiumhydroxide

Analyticalpurity

ShanghaiMcLeanBioc