EC AFM资料说明指南.pdf

NTEGRAforEC

PRESENTATION

Application

Purpose:

In-situcontrol/modificationofthesurfacemorphology

ofsinglecrystalandpolycrystalelectrodes(samples)

duringelectrochemicalprocess(insitu)inelectrolyte

solutionstogetherwithSTM(maxresolution–

atomic)andAFM.

BasicPrinciples

BasicWorkingSchemeCyclicvoltammetryofPt(111)in

0.05MHSO+1mMCuSOsolution

244

1.Sample5.ElectrolyticSolution

2.CCounterElectrode6.CCell

3.ReferenceElectrode7.CellBase

4.STMProbe

ElectrochemicalCell

•Cellmaterial:Teflon

•PlPlatftform:StStanddarddorththogonall

•Maxsize:∅35×10mm

•Argonblowsystem

1

6

2

3

1.WorkingElectrode(sample)4

22.CCellllBBase88

5

3.Platform

4.Cell

5.ElectrodeHolder

66.FiFixiingRiRing

7.TeflonTubeforGas(Ar)Input

8.Heating/coolingunit

77

BipotentiostatSoftware

Bipotentiostat(possibilitytouseexternal)

•OutputComplianceVoltage:±15V

•Applied