铜基红外吸收涂层的制备工艺研究.pdfVIP

HotWorkingTechnology2018，Vo1．47，No．2O

铜基红外吸收涂层的制备工艺研究

乐丽珠，王会玲2张宏坤2，徐正奎2，黄攀3’韩晶

(1．昆明物理研究所，云南昆明650223；2．昆明北方红外技术股份有限公司，云南昆明650223；3．云南北方驰宏光

电有限公司．云南昆明650223)

摘要：红外吸收涂层具有优异的红外吸收能力和抗热震性能而广泛应用于红外探测领域。对铜基红外吸收涂层

的制备关键T艺进行了研究，重点介绍红外吸收基料制备T艺和涂层制备_T艺．同时对铜基红外吸收涂层的红外辐射

性能、微观形貌(SEM)glX射线衍射(XRD)图进行了分析。结果表明：红外吸收基料的配方为45gSiC、20g石墨粉、35g

Fe2()．采用N：气氛保护、烧结温度为分段式升温时．基料的透过率低。吸收率高；铜基红外吸收涂层表面存在结晶体，

无裂纹，涂层巾产生rFeSi、SiO等新物相，新物相的产生提高了涂层的红外辐射性能。

关键词：红外吸收涂层；制备工艺；红外辐射性能

Dol：10．14158／j．cnki．1O01-3814．2018．20．041

中图分类号：TG174．4文献标识码：A文章编号：1001—3814(2018)20．0164．05

StudyonPreparationProcessOfC0pper—basedInfraredAbsorptionCoatings

LELizhu，WANGHuiling2，ZHANGHongkun，XUZhengkui，HUANGPan，HANJing

(1．KunmingInstituteofPhysics，Kunming650223，China；2．KunmingNoahInfraredTechnologyCo．，Ltd．，Kunming

650223，China；3．YunnanKiro-ChPhotonicsCo．，Ltd．，Kunming650223，China)

Abstract：Infraredabsorbingcoatingiswidelyusedininfrareddetectionforitsexcellentinfraredabsorptionandthermal

shockresistance．Thekeytechnologiesofrthep~pamtionofcopper-basedinrfaredabsorbingcoatingswerestudied．The

preparationprocessofinrfaredabsorptionbasematerialsandcoatingwasintroduced．Atthesametime，theinfraredradiation

properties，microscopicmoprholoyg(SEM)andX—mydiffraction(XRD)paRemofthecopper-basedinrfaredabsorbing

coatingswereanalyzed．Theresultsshowthattheformulaofinrfaredabsorptionbasematerialis45gSiC，20ggraphim

powder，35gFe203；whenhtesinteringtemperatureissegmented，htebasematerialhaslowtransmittanceandhig【habsoprtion

ratewithN2atmosphereprotection．Thesurfaceofhtecopper-basedinrfaredabsorbingcoatinghascrystalsandnocracks．

NewphasessuchasFe3SiandSiO2apperainthecoating．Theappearanceofnewphasesenhanceshteinrfaredradiation

propertiesofthecoating．

Keywords：infr